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网站主页CAS数据库列表 968-81-0更多图谱醋磺环已脲(968-81-0)红外图谱(IR1)

醋磺环已脲

产品名称 醋磺环已脲

CAS号968-81-0

分子式C15H20N2O4S

分子量324.4

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  • Mass

    MS-IW-3427          
    p-acetyl-N-(cyclohexylcarbamoyl)benzenesulfonamide
    C15H20N2O4S         (Mass of molecular ion:    324)
    

       Source Temperature: 150 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          15.0       1.1
          27.0       2.0
          28.0       3.8
          29.0       1.4
          30.0       3.8
          38.0       1.2
          39.0       3.5
          41.0       2.9
          42.0       3.1
          43.0      27.5
          44.0       1.3
          50.0       7.8
          51.0       2.9
          52.0       1.3
          53.0       1.1
          54.0       1.4
          55.0       1.9
          56.0      68.6
          57.0       3.6
          62.0       1.0
          63.0       2.5
          64.0       1.5
          65.0       1.7
          67.0       1.6
          70.0       5.4
          74.0       3.2
          75.0      11.7
          76.0      10.8
          77.0       4.1
          78.0       1.1
          81.0       1.1
          82.0       1.3
          89.0       1.2
          90.0       2.6
          91.0       7.4
          92.0       2.4
          98.0       2.7
          99.0      11.9
         104.0       6.7
         107.0       1.3
         119.0       6.1
         120.0       9.1
         121.0       1.1
         139.0       1.9
         141.0       1.8
         152.0       1.1
         182.0       7.1
         183.0       4.0
         184.0       2.7
         210.0     100.0
         211.0      10.1
         212.0       5.7
         225.0      14.5
         226.0       1.7
         243.0       1.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C15 H20 N2 O4 S 0.040 g : 0.5 ml DMSO-d6
    p-acetyl-N-(cyclohexylcarbamoyl)benzenesulfonamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.56 B 8.150 C 8.041 D 6.45 E 3.282 F 2.649 G 1.66 J 1.59 K 1.485 L 1.20 M 1.12 N 1.10 J(D,E)=8.0HZ ASSIGNED BY C-H AND H-H COSY.

         Hz     ppm     Int.
    

       3262.18   8.163    189
       3260.19   8.158     68
       3255.46   8.146     79
       3253.33   8.141    270
       3251.65   8.137     50
       3218.84   8.055     46
       3217.16   8.050    284
       3215.18   8.045     80
       3210.45   8.034     67
       3208.47   8.029    190
       3206.63   8.024     30
       2582.09   6.461     31
       2574.31   6.442     32
       1058.65   2.649   1000
        666.96   1.669     45
        662.38   1.658     37
        656.89   1.644     44
        654.60   1.638     44
        644.99   1.614     32
        644.38   1.613     31
        641.63   1.606     37
        637.66   1.596     34
        632.32   1.583     42
        628.66   1.574     48
        490.26   1.227     37
        478.67   1.198     48
        465.85   1.166     42
        463.56   1.160     47
        461.43   1.155     46
        451.35   1.130     63
        441.89   1.106     49
        439.00   1.099     50
    

in DMSO-d6



KBr disc



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