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网站主页CAS数据库列表 7781-49-9更多图谱5-(4-碘苯)-1-(4-硝基苯)-3-苯基甲(7781-49-9)Raman光谱

5-(4-碘苯)-1-(4-硝基苯)-3-苯基甲

产品名称 5-(4-碘苯)-1-(4-硝基苯)-3-苯基甲

CAS号7781-49-9

分子式C19H14IN5O2

分子量471.25

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  • Mass

    MS-NW-9117          
    5-(p-iodophenyl)-1-(p-nitrophenyl)-3-phenylformazan
    C19H14IN5O2         (Mass of molecular ion:    471)
    

       Source Temperature: 210 °C
       Sample Temperature: 190 °C
       Direct, 75 eV
    

          17.0       1.6
          18.0       9.0
          27.0       1.9
          28.0      14.9
          29.0       1.1
          30.0      82.6
          37.0       1.6
          38.0       4.3
          39.0      14.0
          40.0       1.4
          41.0       3.6
          43.0       1.1
          50.0      17.2
          51.0      14.6
          52.0       8.2
          53.0       3.2
          57.0       1.0
          58.0       1.4
          62.0       4.3
          63.0      29.5
          64.0      27.7
          65.0      18.7
          66.0       2.4
          74.0       4.9
          75.0       8.4
          76.0      42.4
          77.0      36.3
          78.0       4.6
          79.0       4.9
          80.0       3.8
          81.0       1.7
          83.0       1.0
          88.0       3.0
          89.0       5.0
          90.0      39.9
          91.0      52.9
          92.0      21.1
          93.0       3.0
         102.0       1.6
         103.0      28.4
         104.0      18.8
         105.0      21.1
         106.0       3.8
         107.0       3.7
         108.0       3.4
         115.0       1.5
         118.0       1.1
         120.0       1.1
         121.0       2.9
         122.0       4.1
         123.0       2.3
         127.0       2.0
         128.0       2.5
         136.0       3.7
         137.0      21.2
         138.0       8.7
         139.0       6.1
         140.0       4.5
         141.0       1.0
         145.0       2.5
         150.0       1.5
         151.0       1.8
         152.0       2.2
         153.0       1.2
         154.0       1.4
         160.0       1.4
         163.0       2.9
         164.0       4.0
         165.0       8.9
         166.0      16.6
         167.0      11.7
         168.0       2.3
         178.0       1.2
         179.0       5.0
         180.0       1.7
         181.0       1.5
         182.0       1.8
         183.0       1.6
         191.0       6.9
         192.0       4.3
         193.0      11.2
         194.0     100.0
         195.0      17.0
         196.0       1.6
         203.0      16.7
         204.0       8.8
         209.0       2.5
         210.0       1.8
         211.0       1.3
         212.0       2.0
         217.0      26.9
         218.0      90.7
         219.0      25.3
         220.0       2.1
         223.0      10.2
         224.0       1.8
         225.0       1.9
         231.0       3.5
         235.5       1.9
         239.0      19.3
         240.0      61.8
         241.0      23.0
         242.0       3.5
         249.0       5.1
         256.0       3.5
         268.0       1.8
         292.0       1.0
         294.0       1.7
         306.0       4.3
         307.0       1.3
         310.0       4.7
         320.0      37.0
         321.0       6.8
         322.0       1.4
         324.0       1.8
         330.0      11.2
         337.0       1.6
         339.0       1.1
         340.0      10.6
         341.0       1.6
         342.0       1.2
         345.0       1.0
         349.0       2.1
         353.0       1.0
         362.0       1.1
         421.0       1.9
         441.0       1.4
         442.0       1.1
         443.0      15.9
         444.0       3.5
         471.0      24.0
         472.0       5.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C19 H14 I N5 O2 saturated in DMSO-d6
    5-(p-iodophenyl)-1-(p-nitrophenyl)-3-phenylformazan
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.7 B 8.245 C 8.018 D 7.892 E 7.777 F 7.672 G 7.48 to 7.43 ASSIGNED BY C-H AND H-H COSY.

         Hz     ppm     Int.
    

       3257.62   8.152    164
       3256.88   8.150    146
       3255.97   8.148    127
       3255.05   8.145    127
       3250.47   8.134    126
       3249.01   8.130    159
       3224.65   8.069    122
       3214.21   8.043    126
       3209.44   8.031    594
       3205.96   8.022    272
       3205.60   8.022    270
       3201.02   8.010    757
       3181.79   7.962    146
       3163.47   7.916    164
       3157.79   7.902    719
       3153.58   7.891    331
       3153.03   7.890    332
       3149.73   7.882    573
       3144.97   7.870    174
       3142.59   7.864    122
       3119.51   7.806    128
       3118.96   7.805    137
       3117.31   7.801    175
       3111.82   7.787    577
       3111.45   7.786    580
       3108.15   7.778    369
       3104.67   7.769    635
       3100.28   7.758    169
       3098.99   7.755    137
       3096.98   7.750    132
       3096.43   7.748    131
       3095.33   7.746    143
       3094.41   7.743    125
       3089.10   7.730    122
       3088.55   7.729    142
       3088.00   7.727    136
       3087.64   7.726    131
       3070.60   7.684    605
       3066.57   7.674    289
       3066.02   7.672    286
       3061.81   7.662    606
       3054.67   7.644    135
       3053.94   7.642    130
       3053.57   7.641    132
       3052.65   7.639    136
       3052.29   7.638    140
       3051.74   7.637    143
       3051.19   7.635    143
       3050.64   7.634    140
       3050.09   7.632    127
       3044.78   7.619    136
       3044.23   7.618    137
       3043.68   7.616    130
       3043.31   7.615    128
       3042.21   7.613    125
       3041.66   7.611    123
       3041.11   7.610    125
       3039.46   7.606    123
       3038.92   7.604    127
       3038.37   7.603    127
       3037.45   7.601    128
       3037.08   7.600    127
       3036.35   7.598    126
       3035.98   7.597    122
       3035.25   7.595    123
       3034.89   7.594    122
       3033.42   7.591    126
       3033.05   7.590    130
       3032.69   7.589    123
       3032.14   7.587    126
       3000.27   7.508    123
       2999.53   7.506    125
       2997.15   7.500    199
       2995.14   7.495    249
       2994.59   7.494    252
       2992.21   7.488    310
       2991.84   7.487    312
       2991.29   7.485    312
       2986.16   7.472    711
       2979.02   7.455   1000
       2974.81   7.444    353
       2973.16   7.440    309
       2972.79   7.439    305
       2967.66   7.426    140
       2966.56   7.423    159
       2965.10   7.420    122
    

in DMSO-d6



KBr disc



nujol mull