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4-氯-5-甲基-2-硝基苯酚

产品名称 4-氯-5-甲基-2-硝基苯酚

CAS号7147-89-9

分子式C7H6ClNO3

分子量187.58

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  • Mass

    MS-IW-0709          
    4-chloro-6-nitro-m-cresol
    C7H6ClNO3           (Mass of molecular ion:    187)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          28.0       1.1
          30.0       1.0
          39.0       2.0
          50.0       2.1
          51.0       7.6
          52.0       1.2
          53.0       2.5
          63.0       1.6
          65.0       2.6
          73.0       1.1
          75.0       2.3
          76.0       1.1
          77.0      21.8
          78.0       3.5
          87.0       1.0
          89.0       1.2
          90.0       2.3
          94.0       1.2
          99.0       1.0
         105.0       1.1
         111.0       1.1
         112.0       2.9
         113.0       4.0
         114.0       1.2
         115.0       1.3
         129.0       4.5
         131.0       1.5
         139.0       1.4
         141.0       7.9
         142.0       2.0
         143.0       2.5
         157.0       4.5
         159.0       1.5
         170.0       4.7
         172.0       1.5
         187.0     100.0
         188.0       8.1
         189.0      32.6
         190.0       2.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H6 Cl N O3 0.041 g : 0.5 ml CDCl3
    4-chloro-6-nitro-m-cresol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.43 B 8.078 C 7.047 D 2.417

         Hz     ppm     Int.
    

       4170.33  10.435    622
       3228.49   8.079    414
       2817.10   7.049    281
       2816.73   7.048    291
       2816.37   7.048    278
        966.57   2.419    983
        966.20   2.418   1000
        965.84   2.417    943
    

in CDCl3



KBr disc



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