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网站主页CAS数据库列表 68922-17-8更多图谱1,1′-亚甲基双(3-甲基哌啶)(68922-17-8)红外图谱(IR1)

1,1′-亚甲基双(3-甲基哌啶)

产品名称 1,1′-亚甲基双(3-甲基哌啶)

CAS号68922-17-8

分子式C13H26N2

分子量210.36

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  • Mass

    MS-NW-6451          
    1,1'-methylenebis(3-methylpiperidine)
    C13H26N2            (Mass of molecular ion:    210)
    

       Source Temperature: 240 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       2.7
          18.0       1.4
          27.0       5.4
          28.0       6.9
          29.0       6.7
          30.0      16.2
          39.0       6.7
          40.0       1.7
          41.0      15.2
          42.0      20.2
          43.0      12.3
          44.0      30.6
          45.0       1.0
          53.0       1.9
          54.0       1.7
          55.0       7.8
          56.0      12.3
          57.0      13.8
          58.0       6.0
          67.0       2.5
          68.0       4.4
          69.0       6.5
          70.0       7.9
          71.0       3.5
          80.0       1.1
          81.0       1.5
          82.0       3.4
          83.0       1.4
          84.0      11.6
          85.0       1.0
          93.0       1.0
          94.0       2.1
          96.0       6.4
          97.0       1.3
          98.0      13.3
          99.0      12.4
         100.0       1.1
         108.0       2.2
         109.0       1.9
         110.0       3.4
         111.0       8.7
         112.0     100.0
         113.0      10.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H26 N2 0.04 ml : 0.5 ml CDCl3
    1,1'-methylenebis(3-methylpiperidine)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.89 B 2.86 C 2.850 D 1.846 E 1.68 F 1.65 to 1.530 G 1.56 J 1.54 K 0.85 L 0.852 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       1160.64   2.905    110
       1158.94   2.900     96
       1157.23   2.896     85
       1149.66   2.877    230
       1142.82   2.860    141
       1139.16   2.851    845
        750.61   1.879     78
        747.56   1.871     80
        739.38   1.851    153
        736.21   1.843    149
        728.15   1.822     84
        724.85   1.814     80
        685.06   1.715     40
        683.11   1.710     69
        681.64   1.706     89
        679.69   1.701     97
        678.10   1.697    102
        676.39   1.693     78
        674.44   1.688     69
        672.73   1.684     61
        670.53   1.678     71
        669.07   1.675     97
        667.24   1.670    126
        665.77   1.666    127
        663.82   1.662    131
        661.13   1.655     87
        657.59   1.646     91
        653.93   1.637    109
        650.76   1.629    130
        647.58   1.621    166
        644.29   1.613    149
        641.72   1.606    124
        640.14   1.602    136
        638.79   1.599    191
        637.57   1.596    171
        635.50   1.591    199
        634.40   1.588    238
        631.59   1.581    342
        627.93   1.572    150
        624.02   1.562    102
        621.34   1.555    259
        616.09   1.542    151
        611.21   1.530    132
        608.28   1.523     72
        607.06   1.519     58
        604.37   1.513    102
        603.27   1.510     77
        600.46   1.503     57
        599.37   1.500     42
        595.09   1.490     30
        591.19   1.480     45
        367.31   0.920     54
        361.21   0.904     85
        356.93   0.894     74
        349.12   0.874    165
        343.87   0.861   1000
        337.65   0.845    935
        332.76   0.833    114
        326.42   0.817     50
        322.14   0.807     37
    

in CDCl3



liquid film



4880 A,200 M,liquid