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网站主页CAS数据库列表 6294-17-3更多图谱1-溴-6-氯己烷(6294-17-3)质谱(MS)

1-溴-6-氯己烷

产品名称 1-溴-6-氯己烷

CAS号6294-17-3

分子式C6H12BrCl

分子量199.52


  • Mass

    MS-NW-7489          
    1-bromo-6-chlorohexane
    C6H12BrCl           (Mass of molecular ion:    198)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.0
          26.0       2.5
          27.0      24.0
          28.0       4.4
          29.0      18.0
          38.0       1.1
          39.0      16.9
          40.0       3.5
          41.0      59.8
          42.0      13.5
          43.0      33.2
          44.0       1.1
          49.0       3.0
          51.0       1.5
          53.0       5.4
          54.0       5.1
          55.0     100.0
          56.0      15.5
          57.0      11.2
          62.0       1.3
          63.0       3.8
          65.0       1.3
          67.0      12.1
          68.0       1.1
          69.0      17.3
          70.0       1.2
          75.0       1.3
          76.0       1.2
          77.0       6.7
          79.0       2.1
          81.0       2.9
          82.0      17.5
          83.0      96.1
          84.0       6.5
          90.0       2.8
          91.0       2.5
          92.0       1.1
          93.0       1.1
          95.0       1.0
         107.0       3.8
         109.0       3.6
         118.0       6.5
         119.0       3.7
         120.0       2.4
         121.0       1.2
         134.0       1.2
         135.0       2.0
         136.0       1.3
         137.0       1.8
         162.0       1.8
         164.0       1.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H12 Br Cl 0.05 ml : 0.5 ml CDCl3
    1-bromo-6-chlorohexane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.531 B 3.412 C 1.81 D 1.48

         Hz     ppm     Int.
    

        330.38   3.689     31
        329.63   3.681     30
        329.25   3.677     32
        323.50   3.613    386
        321.00   3.585    110
        317.13   3.541    928
        312.50   3.490    499
        310.69   3.470    636
        306.00   3.417   1000
        299.31   3.343    606
        295.88   3.304     40
        295.00   3.294     36
        294.44   3.288     33
        294.13   3.285     31
        182.81   2.042     44
        181.56   2.028     60
        180.50   2.016     62
        180.31   2.014     62
        179.00   1.999     71
        174.56   1.950    194
        173.63   1.939    200
        167.19   1.867    369
        161.00   1.798    402
        156.81   1.751    244
        155.13   1.733    275
        154.19   1.722    274
        151.94   1.697    183
        151.63   1.694    184
        149.94   1.675    153
        149.38   1.668    155
        148.00   1.653    168
        144.88   1.618    166
        142.94   1.597    166
        137.69   1.538    489
        134.81   1.506    498
        133.69   1.493    499
        131.19   1.465    589
        128.31   1.433    365
        127.00   1.419    404
        124.56   1.391    216
        123.38   1.378    213
        119.13   1.331     66
        118.38   1.322     63
        117.63   1.314     56
        115.94   1.295     40
        115.44   1.289     38
        115.00   1.285     35
        113.75   1.271     31
    

in CDCl3



liquid film