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网站主页CAS数据库列表 620-95-1更多图谱3-苄基吡啶(620-95-1)质谱(MS)

3-苄基吡啶

产品名称 3-苄基吡啶

CAS号620-95-1

分子式C12H11N

分子量169.22

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  • Mass

    MS-IW-3672          
    3-benzylpyridine
    C12H11N             (Mass of molecular ion:    169)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          38.0       1.1
          39.0       7.0
          41.0       1.0
          50.0       2.5
          51.0       6.0
          52.0       1.4
          57.5       1.6
          62.0       1.7
          63.0       6.0
          64.0       2.6
          65.0       9.9
          66.0       1.1
          69.5       1.0
          70.0       1.2
          70.5       1.5
          71.5       3.0
          74.0       1.1
          75.0       1.2
          76.0       1.1
          77.0       2.7
          78.0       1.1
          83.5       6.7
          84.0       1.1
          89.0       4.4
          90.0       2.7
          91.0      14.9
          92.0       3.6
         102.0       1.3
         114.0       1.0
         115.0       9.6
         116.0       1.6
         128.0       1.0
         139.0       5.0
         140.0       2.8
         141.0       9.5
         142.0       2.5
         154.0       2.1
         166.0       4.6
         167.0      29.7
         168.0     100.0
         169.0      94.3
         170.0      11.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H11 N 0.035 g : 0.5 ml CDCl3
    3-benzylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.506 B 8.452 C 7.445 D 7.291 E 7.214 F 7.19 G 7.17 J 3.962

         Hz     ppm     Int.
    

       3399.41   8.506    171
       3379.76   8.457    121
       3375.85   8.448    124
       2982.06   7.462    112
       2980.35   7.458    170
       2979.74   7.456    167
       2978.03   7.452    113
       2974.24   7.443    134
       2972.53   7.438    198
       2971.92   7.437    195
       2970.21   7.433    130
       2923.58   7.316    129
       2922.49   7.313    212
       2920.90   7.309     94
       2917.24   7.300    140
       2915.53   7.296    575
       2914.18   7.292    295
       2909.30   7.280    191
       2907.96   7.277    465
       2905.88   7.272     98
       2891.72   7.236    106
       2890.26   7.232    211
       2888.92   7.229    149
       2885.13   7.220     80
       2882.93   7.214    276
       2880.62   7.208     84
       2875.61   7.196    233
       2874.27   7.192     94
       2869.38   7.180    478
       2868.65   7.178    532
       2868.04   7.177    626
       2865.84   7.171    159
       2862.55   7.163    281
       2861.94   7.162    315
       2861.21   7.160    397
       2860.60   7.158    371
       2859.86   7.156    299
       2857.79   7.151     61
       1583.50   3.963   1000
    

in CDCl3



KBr disc



liquid film



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