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网站主页CAS数据库列表 580-51-8更多图谱间羟基联苯(580-51-8)质谱(MS)

间羟基联苯

产品名称 间羟基联苯

CAS号580-51-8

分子式C12H10O

分子量170.21

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  • Mass

    MS-NW-4470          
    biphenyl-3-ol
    C12H10O             (Mass of molecular ion:    170)
    

       Source Temperature: 230 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          39.0       2.9
          50.0       1.5
          51.0       2.5
          55.0       1.9
          57.5       1.3
          62.0       1.2
          63.0       3.3
          65.0       1.3
          70.0       1.4
          72.0       1.6
          74.0       1.2
          75.0       1.4
          76.0       2.5
          77.0       2.0
          84.0       2.7
          85.0       3.3
          89.0       1.7
         102.0       1.5
         115.0      11.0
         116.0       1.6
         139.0       4.1
         140.0       1.4
         141.0      17.9
         142.0       3.2
         144.0       1.1
         151.0       1.3
         152.0       2.1
         153.0       1.3
         168.0       1.9
         169.0       8.5
         170.0     100.0
         171.0      13.1
         172.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 O 0.041 g : 0.5 ml CDCl3
    biphenyl-3-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.64 to 7.14 B 7.17 C 7.04 D 6.80 E 5.05

         Hz     ppm     Int.
    

        681.19   7.606    212
        680.06   7.594    147
        679.50   7.588    174
        677.75   7.568    313
        676.06   7.549    311
        674.88   7.536    202
        674.00   7.526    306
        672.75   7.512    702
        670.88   7.491   1000
        668.44   7.464    426
        666.88   7.447    399
        666.19   7.439    305
        664.13   7.416    675
        663.25   7.406    785
        661.00   7.381    743
        659.06   7.359    481
        657.94   7.347    765
        656.00   7.325    876
        653.75   7.300    603
        653.19   7.294    531
        652.13   7.282    150
        646.38   7.218    597
        645.75   7.211    744
        643.50   7.186    829
        641.94   7.168    578
        640.38   7.151     59
        637.56   7.119    123
        635.94   7.101    272
        634.25   7.082    149
        632.81   7.066    314
        632.25   7.060    409
        631.19   7.048    274
        630.25   7.038    468
        629.63   7.031    455
        628.75   7.021    342
        628.13   7.014    313
        614.13   6.858    387
        612.44   6.839    332
        611.56   6.829    319
        609.94   6.811    257
        606.81   6.776    281
        605.06   6.756    259
        604.25   6.747    242
        602.56   6.729    212
        452.19   5.050    395
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder