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网站主页CAS数据库列表 506-43-4更多图谱顺、顺-9,12-十八碳二烯醇(506-43-4)质谱(MS)

顺、顺-9,12-十八碳二烯醇

产品名称 顺、顺-9,12-十八碳二烯醇

CAS号506-43-4

分子式C18H34O

分子量266.46

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  • Mass

    MS-IW-4198          
    cis,cis-9,12-octadecadien-1-ol
    C18H34O             (Mass of molecular ion:    266)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       2.6
          27.0       3.5
          28.0       4.4
          29.0       8.8
          31.0       3.6
          32.0       1.4
          39.0       4.6
          41.0      29.9
          42.0       3.7
          43.0      21.3
          44.0       1.3
          53.0       5.0
          54.0      39.3
          55.0      50.2
          56.0       6.4
          57.0      11.4
          58.0       5.4
          59.0       2.5
          65.0       3.3
          66.0       8.5
          67.0     100.0
          68.0      54.6
          69.0      31.9
          70.0       6.2
          71.0       8.7
          72.0       1.2
          77.0       5.6
          78.0       3.8
          79.0      33.5
          80.0      30.1
          81.0      95.4
          82.0      77.2
          83.0      22.8
          84.0       6.2
          85.0       6.1
          86.0       1.3
          91.0       5.9
          92.0       1.8
          93.0      23.1
          94.0      16.9
          95.0      67.8
          96.0      59.3
          97.0      17.9
          98.0      14.1
          99.0       2.6
         105.0       1.6
         107.0      13.4
         108.0       9.7
         109.0      29.3
         110.0      29.5
         111.0       9.1
         112.0       4.5
         121.0      21.4
         122.0       7.8
         123.0      12.1
         124.0      14.4
         125.0       3.5
         126.0       1.6
         135.0      13.2
         136.0       6.4
         137.0       6.2
         138.0       7.5
         139.0       1.8
         140.0       1.1
         149.0       5.5
         150.0       3.2
         151.0       2.8
         152.0       4.5
         153.0       1.2
         163.0       2.4
         164.0       1.3
         165.0       1.5
         166.0       3.0
         177.0       1.2
         180.0       1.1
         248.0       2.2
         266.0       5.8
         267.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H34 O 0.05 ml : 0.5 ml CDCl3
    cis,cis-9,12-octadecadien-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.36 B 3.619 C 2.773 D 2.050 E 1.95 F 1.558 G 1.26 J 0.891

         Hz     ppm     Int.
    

       2151.37   5.384    117
       2146.61   5.372    213
       2146.00   5.370    205
       2144.41   5.366    239
       2140.75   5.357    353
       2138.67   5.352    167
       2135.25   5.343    333
       2128.54   5.327    136
       2127.56   5.324    125
       1453.25   3.637    327
       1446.53   3.620    643
       1439.82   3.603    342
       1115.23   2.791    147
       1108.52   2.774    308
       1102.17   2.758    178
        829.83   2.077    164
        823.12   2.060    436
        816.16   2.043    455
        809.45   2.026    186
        780.27   1.953     71
        629.76   1.576    121
        622.80   1.559    184
        615.60   1.541    155
        548.71   1.373    221
        542.60   1.358    372
        541.50   1.355    353
        535.16   1.340    458
        523.68   1.311    984
        520.87   1.304   1000
        514.16   1.287    384
        511.35   1.280    252
        507.81   1.271    135
        363.04   0.909    293
        356.20   0.892    715
        349.24   0.874    321
    

in CDCl3



liquid film