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网站主页CAS数据库列表 3438-48-0更多图谱4-苯基嘧啶(3438-48-0)红外图谱(IR1)

4-苯基嘧啶

产品名称 4-苯基嘧啶

CAS号3438-48-0

分子式C10H8N2

分子量156.18

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  • Mass

    MS-NW-7110          
    4-phenylpyrimidine
    C10H8N2             (Mass of molecular ion:    156)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          26.0       7.6
          27.0       1.7
          28.0       4.6
          37.0       1.0
          38.0       1.7
          39.0       3.8
          49.0       1.0
          50.0       9.6
          51.0      13.5
          52.0       8.8
          53.0      11.0
          61.0       1.1
          62.0       2.1
          63.0       4.1
          64.0       1.2
          74.0       4.7
          75.0       6.1
          76.0      11.9
          77.0       9.0
          78.0       4.1
          79.0       1.9
         101.0       3.8
         102.0      43.1
         103.0      17.7
         104.0       5.1
         128.0       6.5
         129.0      59.1
         130.0       6.8
         149.0       1.2
         155.0       9.2
         156.0     100.0
         157.0      11.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H8 N2 0.039 g : 0.5 ml CDCl3
    4-phenylpyrimidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.267 B 8.746 C 8.083 D 7.697 E 7.60 to 7.40 J(A,D)=1.4HZ. J(B,D)=5.4HZ.

         Hz     ppm     Int.
    

        830.56   9.274    503
        829.44   9.262    473
        786.13   8.778    457
        780.81   8.719    502
        731.44   8.168     86
        729.25   8.143    400
        727.69   8.126    262
        726.25   8.110    353
        725.00   8.096    324
        723.56   8.080    364
        722.56   8.068    412
        720.81   8.049    296
        719.44   8.034    526
        715.31   7.987     91
        692.63   7.734    459
        691.19   7.718    452
        687.19   7.673    424
        685.81   7.658    414
        678.94   7.581    139
        676.69   7.556    342
        675.19   7.539   1000
        673.63   7.522    498
        671.94   7.503    896
        670.75   7.490    488
        670.00   7.482    394
        668.56   7.465    843
        667.38   7.452    231
        666.75   7.445    211
        666.31   7.440    202
        664.56   7.421    119
    

in CDCl3



KBr disc



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