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网站主页CAS数据库列表 2362-61-0更多图谱反式-2-苯基-1-环已醇(2362-61-0)核磁图(13CNMR)

反式-2-苯基-1-环已醇

产品名称 反式-2-苯基-1-环已醇

CAS号2362-61-0

分子式C12H16O

分子量176.25

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  • Mass

    MS-NW-8911          
    trans-2-phenyl-1-cyclohexanol
    C12H16O             (Mass of molecular ion:    176)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.6
          27.0       5.3
          28.0       1.6
          29.0       5.6
          31.0       1.6
          39.0       7.3
          41.0      10.2
          42.0       1.2
          43.0       4.5
          44.0       3.0
          50.0       1.2
          51.0       6.1
          52.0       1.9
          53.0       2.5
          55.0       5.1
          57.0      21.3
          58.0       1.2
          63.0       2.8
          64.0       1.3
          65.0       8.5
          66.0       3.4
          67.0       9.8
          68.0       1.0
          69.0       1.2
          70.0       3.0
          71.0      10.4
          76.0       1.2
          77.0      12.9
          78.0      13.2
          79.0       7.9
          80.0       4.0
          83.0       1.7
          84.0       3.1
          85.0      10.5
          89.0       2.8
          90.0       1.2
          91.0     100.0
          92.0      44.7
          93.0       3.6
          98.0      18.6
          99.0       1.3
         102.0       2.1
         103.0       9.6
         104.0      44.0
         105.0      18.6
         106.0       2.1
         107.0       1.7
         115.0      14.2
         116.0       4.4
         117.0      40.5
         118.0       5.5
         119.0       1.4
         120.0       3.5
         127.0       1.5
         128.0       4.8
         129.0      23.8
         130.0      42.2
         131.0       7.5
         132.0      13.0
         133.0       7.9
         134.0       1.1
         143.0      11.5
         144.0       1.5
         145.0       1.3
         148.0       1.0
         157.0       1.9
         158.0      12.8
         159.0       1.9
         176.0      60.7
         177.0       8.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H16 O 0.05 g : 0.5 ml CDCl3
    trans-2-phenyl-1-cyclohexanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.284 B 7.21 C 7.19 D 3.582 E 2.377 F 2.060 G 1.82 K 1.72 L 1.49 M 1.38 N 1.35 P 1.28

         Hz     ppm     Int.
    

       2919.80   7.306    234
       2918.95   7.304    340
       2917.48   7.301    148
       2912.35   7.288    627
       2911.50   7.286    723
       2906.13   7.272    278
       2904.30   7.268    730
       2885.62   7.221    633
       2884.03   7.217   1000
       2881.96   7.212    303
       2880.00   7.207    426
       2878.91   7.204    483
       2878.05   7.202    501
       2877.20   7.200    663
       2875.98   7.197    504
       2873.66   7.191    298
       2871.58   7.186    479
       2869.38   7.180    154
       2865.84   7.171    149
       2864.38   7.168    214
       2863.04   7.164    116
       1444.09   3.614    108
       1439.70   3.603    103
       1433.84   3.588    236
       1429.69   3.578    192
       1423.83   3.563    145
       1419.56   3.553    100
        963.01   2.410    122
        959.47   2.401    130
        953.00   2.385    135
        950.68   2.379    207
        947.27   2.371    157
        940.80   2.355    137
        937.26   2.346    136
        830.57   2.079    132
        828.37   2.073    198
        826.54   2.069    126
        823.61   2.061    117
        822.51   2.059    106
        819.21   2.050    154
        816.28   2.043    125
        814.82   2.039     90
        735.96   1.842    236
        734.62   1.839    227
        732.67   1.834    241
        729.37   1.826    168
        723.02   1.810    363
        720.83   1.804    362
        708.74   1.774     40
        705.93   1.767     40
        695.92   1.742    252
        691.77   1.731    394
        688.48   1.723    234
        684.94   1.714    210
        682.01   1.707    156
        610.23   1.527     81
        606.57   1.518     56
        597.66   1.496    186
        594.12   1.487    155
        584.11   1.462    179
        581.79   1.456    138
        575.56   1.441     52
        571.66   1.431     96
        568.12   1.422     70
        565.80   1.416     94
        562.74   1.409    115
        559.81   1.401     60
        552.86   1.384    173
        550.42   1.378    262
        546.88   1.369    167
        544.07   1.362    124
        539.67   1.351    453
        536.38   1.343    172
        533.33   1.335    128
        531.01   1.329    154
        527.95   1.322    199
        524.05   1.312    190
        520.51   1.303    147
        514.89   1.289     94
        511.11   1.279    127
        507.69   1.271     94
        498.54   1.248     40
    

in CDCl3



KBr disc



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