图谱信息 供应商 相关产品
网站主页CAS数据库列表 2216-69-5更多图谱1-甲氧基萘(2216-69-5)质谱(MS)

1-甲氧基萘

产品名称 1-甲氧基萘

CAS号2216-69-5

分子式C11H10O

分子量158.2

展开


  • Mass

    MS-NW-5217          
    methyl 1-naphthyl ether
    C11H10O             (Mass of molecular ion:    158)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.6
          28.0       1.1
          39.0       4.3
          50.0       2.7
          51.0       3.4
          62.0       3.5
          63.0       8.1
          64.0       1.5
          65.0       4.1
          74.0       3.0
          75.0       3.7
          76.0       1.5
          77.0       2.7
          79.0       2.4
          86.0       1.5
          87.0       2.1
          88.0       2.2
          89.0       6.8
         101.0       1.4
         113.0       2.4
         114.0       4.0
         115.0      79.7
         116.0       8.1
         126.0       2.7
         127.0       5.4
         128.0       4.9
         129.0       2.2
         143.0      35.6
         144.0       4.3
         157.0       2.0
         158.0     100.0
         159.0      11.7
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C11 H10 O 0.031 g : 0.5 ml CDCl3
    methyl 1-naphthyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.260 B 7.765 C 7.59 to 7.31 D 6.776 E 3.963

         Hz     ppm     Int.
    

        744.88   8.318     35
        744.31   8.311     48
        741.75   8.283     31
        740.44   8.268     32
        738.25   8.244     55
        735.13   8.209     43
        734.50   8.202     58
        701.94   7.838     39
        701.25   7.830     40
        698.38   7.798     61
        696.25   7.775     47
        694.44   7.754     51
        692.31   7.731     75
        691.63   7.723     70
        675.75   7.546     32
        675.19   7.539     30
        672.06   7.505    208
        669.06   7.471    110
        668.44   7.464    108
        666.13   7.438     85
        665.31   7.429    100
        663.00   7.403    302
        662.44   7.397    195
        660.50   7.375    105
        660.06   7.371    102
        658.56   7.354     35
        657.38   7.341    189
        611.19   6.825     70
        608.19   6.791     48
        605.38   6.760     54
        602.44   6.727     52
        355.06   3.965   1000
        354.75   3.962    999
    


  • 1H NMR 399.65 MHz
    C11 H10 O 0.031 g : 0.5 ml CDCl3
    methyl 1-naphthyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.263 B 7.742 C *1 7.43 D *1 7.43 E 7.372 F 7.309 G 6.694 J 3.863 J(F,G)=7.3HZ. J(E,G)=1.0HZ.

         Hz     ppm     Int.
    

       3307.62   8.277     50
       3306.88   8.275     83
       3306.15   8.273     55
       3304.69   8.269     43
       3303.71   8.267     44
       3303.10   8.265     48
       3302.37   8.264     47
       3300.90   8.260     69
       3300.17   8.258     71
       3297.85   8.252     52
       3297.12   8.251     84
       3296.39   8.249     53
       3098.88   7.754     75
       3095.70   7.747     89
       3093.38   7.741     61
       3092.04   7.737     50
       3091.67   7.736     51
       3089.36   7.731     83
       2976.68   7.449     45
       2975.95   7.447     40
       2972.78   7.439    286
       2969.85   7.432    149
       2969.12   7.430    147
       2966.92   7.424    136
       2965.94   7.422    133
       2963.13   7.415    259
       2960.08   7.407     30
       2959.11   7.405     35
       2952.03   7.387     63
       2951.29   7.385     87
       2943.73   7.366    113
       2942.99   7.364    148
       2927.49   7.326    167
       2919.92   7.307    175
       2919.19   7.305    114
       2911.62   7.286     99
       2679.44   6.705    113
       2678.59   6.703    113
       2671.88   6.686    105
       2671.02   6.684    104
       1543.82   3.863   1000
    

in CDCl3



liquid film



4880 A,200 M,liquid