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网站主页CAS数据库列表 2212-05-7更多图谱4-氯苯基缩水甘油醚(2212-05-7)红外图谱(IR2)

4-氯苯基缩水甘油醚

产品名称 4-氯苯基缩水甘油醚

CAS号2212-05-7

分子式C9H9ClO2

分子量184.62

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  • Mass

    MS-NW-8867          
    p-chlorophenyl 2,3-epoxypropyl ether
    C9H9ClO2            (Mass of molecular ion:    184)
    

       Source Temperature: 280 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          15.0       1.1
          26.0       1.5
          27.0      17.6
          28.0       2.0
          29.0      48.2
          30.0       1.2
          31.0      37.6
          37.0       1.2
          38.0       3.8
          39.0       8.3
          41.0       2.6
          43.0       4.2
          49.0       1.2
          50.0       5.7
          51.0       3.9
          53.0       1.3
          55.0       1.8
          57.0      57.1
          58.0       2.1
          61.0       1.6
          62.0       3.5
          63.0      11.6
          64.0       6.8
          65.0      15.5
          66.0       1.2
          73.0      10.1
          74.0       3.4
          75.0      16.5
          76.0       2.8
          77.0       5.7
          85.0       1.7
          89.0       1.4
          91.0       6.3
          92.0       2.2
          93.0       2.6
          99.0      13.2
         100.0       7.8
         101.0       4.8
         102.0       2.8
         111.0      20.9
         112.0       2.0
         113.0      12.9
         114.0       1.1
         115.0       2.1
         119.0       3.9
         125.0       5.6
         127.0       4.9
         128.0     100.0
         129.0       7.8
         130.0      32.4
         131.0       2.2
         141.0      23.5
         142.0       2.0
         143.0       7.8
         153.0       1.0
         154.0      12.2
         155.0       2.0
         156.0       4.1
         184.0      71.5
         185.0       7.2
         186.0      23.4
         187.0       2.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H9 Cl O2 0.039 g : 0.5 ml CDCl3
    p-chlorophenyl 2,3-epoxypropyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.229 B 6.847 C *1 4.206 D *1 3.892 E 3.335 F 2.899 G 2.743

         Hz     ppm     Int.
    

       2897.34   7.250     92
       2893.92   7.242    971
       2891.72   7.236    290
       2889.53   7.231     40
       2887.21   7.225    318
       2884.89   7.219   1000
       2881.47   7.210    105
       2744.02   6.867    102
       2740.60   6.858    973
       2738.40   6.852    284
       2733.89   6.841    278
       2731.57   6.835    851
       2728.15   6.827     83
       1688.60   4.226    282
       1685.55   4.218    284
       1677.49   4.198    331
       1674.56   4.191    334
       1563.72   3.913    316
       1557.98   3.899    331
       1552.73   3.886    268
       1546.88   3.871    281
       1340.82   3.355     94
       1338.01   3.348    170
       1336.67   3.345    122
       1335.08   3.341    203
       1333.86   3.338    192
       1332.28   3.334    180
       1330.93   3.331    210
       1329.35   3.327    114
       1328.13   3.324    175
       1325.20   3.316     98
       1163.33   2.911    343
       1159.18   2.901    385
       1158.45   2.899    442
       1154.30   2.889    382
       1099.85   2.753    346
       1097.17   2.746    346
       1094.97   2.740    304
       1092.29   2.734    294
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,liquid