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2-碘联苯

产品名称 2-碘联苯

CAS号2113-51-1

分子式C12H9I

分子量280.1

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  • Mass

    MS-NW-5428          
    2-iodobiphenyl
    C12H9I              (Mass of molecular ion:    280)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          39.0       2.9
          50.0       4.1
          51.0       5.6
          52.0       1.1
          61.0       1.1
          62.0       2.4
          63.0       5.4
          74.0       4.3
          75.0       5.1
          75.5       2.2
          76.0      12.1
          76.5       4.2
          77.0       4.8
          86.0       1.5
          87.0       2.0
          98.0       1.5
          99.0       1.3
         101.0       1.6
         102.0       1.8
         126.0       5.7
         127.0       4.8
         140.0       3.5
         150.0       4.3
         151.0      14.9
         152.0      57.9
         153.0      53.5
         154.0       7.3
         280.0     100.0
         281.0      13.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H9 I 0.04 ml : 0.5 ml CDCl3
    2-iodobiphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.934 B 7.55 to 7.18 C 7.003 J(A,C)=7.8HZ.

         Hz     ppm     Int.
    

        715.63   7.991    133
        715.13   7.985    138
        714.44   7.978    164
        713.88   7.971    145
        707.81   7.904    151
        707.19   7.897    159
        706.69   7.891    194
        706.06   7.884    165
        670.44   7.486     42
        668.44   7.464     72
        667.25   7.451     75
        665.88   7.436     62
        664.25   7.417     69
        662.50   7.398    191
        661.81   7.390    263
        660.81   7.379    403
        659.69   7.366   1000
        659.06   7.359    720
        658.19   7.350    673
        656.94   7.336    287
        655.88   7.324    316
        655.44   7.319    288
        654.56   7.309    381
        653.44   7.297    407
        653.13   7.293    412
        652.50   7.286    336
        650.94   7.269     62
        650.31   7.262     51
        649.88   7.257     72
        649.06   7.248     55
        648.31   7.239     83
        647.81   7.234     85
        646.31   7.217     30
        645.50   7.208     38
        644.81   7.200    111
        634.69   7.087    186
        631.88   7.056    129
        628.38   7.017    123
        626.88   7.000    154
        625.56   6.985    108
        623.94   6.967    108
        620.69   6.931    111
        617.75   6.898     92
    

in CDCl3



liquid film