-
MassMS-IW-4852 4-methylphthalic anhydride C9H6O3 (Mass of molecular ion: 162)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.0 28.0 1.9 37.0 2.4 38.0 3.1 39.0 9.0 40.0 2.2 43.0 5.5 43.5 1.4 44.0 2.7 44.5 2.8 45.0 8.4 49.0 1.3 50.0 6.8 51.0 5.2 59.0 1.7 61.0 4.1 62.0 9.8 63.0 19.9 64.0 8.2 73.0 1.0 74.0 3.8 75.0 2.7 77.0 1.0 85.0 1.8 86.0 3.1 87.0 2.5 88.0 1.3 89.0 42.1 90.0 62.8 91.0 6.6 118.0 100.0 119.0 10.4 136.0 1.6 162.0 47.5 163.0 5.0
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C9 H6 O3 0.037 g : 0.5 ml DMSO-d6 4-methylphthalic anhydride 
Assign. Shift(ppm)
A 7.961 B 7.907 C 7.816 D 2.536
Hz ppm Int.3186.18 7.973 173 3178.67 7.954 225 3161.64 7.912 150 3160.90 7.910 238 3160.17 7.908 271 3159.44 7.906 246 3158.71 7.904 151 3128.12 7.828 132 3127.38 7.826 154 3126.65 7.824 146 3126.10 7.823 111 3120.42 7.808 98 3119.69 7.807 121 3118.96 7.805 116 3118.23 7.803 94 1013.83 2.537 1000 1009.98 2.528 43
KBr disc
nujol mull
更多供应商
