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网站主页CAS数据库列表 13878-54-1更多图谱(T-4)-双(1-呱啶二硫代羧酸-S,S’)-锌(13878-54-1)核磁图(1HNMR)

(T-4)-双(1-呱啶二硫代羧酸-S,S’)-锌

产品名称 (T-4)-双(1-呱啶二硫代羧酸-S,S’)-锌

CAS号13878-54-1

分子式C12H20N2S4Zn

分子量385.95

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  • Mass

    MS-IW-3532          
    zinc 1-piperidinecarbodithioate
    C12H20N2S4Zn        (Mass of molecular ion:    384)
    

       Source Temperature: 150 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          27.0       5.6
          28.0       6.8
          29.0       4.3
          30.0       3.7
          32.0       2.1
          34.0       1.6
          38.0       1.1
          39.0       6.7
          40.0       1.4
          41.0      32.7
          42.0       9.0
          43.0       3.7
          44.0       2.9
          45.0       3.1
          53.0       2.7
          54.0       4.2
          55.0      16.6
          56.0      12.2
          57.0       3.1
          58.0       1.3
          59.0       3.5
          60.0       2.5
          64.0       1.5
          65.0       1.0
          67.0       6.6
          68.0      13.2
          69.0      45.6
          70.0       3.7
          72.0      17.9
          73.0       1.6
          74.0       1.2
          76.0      21.6
          77.0       3.2
          78.0       2.1
          80.0       1.2
          82.0       4.8
          83.0      10.7
          84.0      39.2
          85.0       5.4
          86.0       2.5
          87.0       1.6
          94.0       1.0
          96.0       9.5
          97.0       1.1
          98.0       3.4
          99.0       2.0
         100.0       1.5
         101.0       1.4
         126.0       3.0
         127.0      21.0
         128.0     100.0
         129.0      17.0
         130.0       5.4
         147.0       1.0
         148.0       1.2
         149.0       1.0
         150.0       1.0
         160.0      17.4
         161.0       7.2
         162.0       2.1
         180.0       3.9
         182.0       2.5
         184.0       1.6
         192.0       1.2
         223.0       1.2
         224.0      12.8
         225.0       9.2
         226.0      11.4
         227.0       7.3
         228.0       8.1
         229.0       4.1
         230.0       1.9
         256.0       3.5
         257.0       1.1
         258.0       2.5
         259.0       1.0
         260.0       1.7
         307.0      10.7
         308.0       1.9
         309.0       7.1
         310.0       2.1
         311.0       4.9
         326.0       1.2
         351.0       4.6
         353.0       3.2
         354.0       1.0
         355.0       2.3
         384.0      45.7
         385.0       8.2
         386.0      34.5
         387.0       9.6
         388.0      22.9
         389.0       4.4
         390.0       4.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H20 N2 S4 Zn 0.035 g : 0.5 ml DMSO-d6
    zinc 1-piperidinecarbodithioate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.01 B 1.60

         Hz     ppm     Int.
    

       1606.81   4.021    378
       1601.44   4.008    617
        640.14   1.602   1000
    

in DMSO-d6



KBr disc



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