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网站主页CAS数据库列表 1210-33-9更多图谱二苯并环庚烯酮基氯(1210-33-9)Raman光谱

二苯并环庚烯酮基氯

产品名称 二苯并环庚烯酮基氯

CAS号1210-33-9

分子式C15H13Cl

分子量228.72

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  • Mass

    MS-IW-9261          
    5-chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene
    C15H13Cl            (Mass of molecular ion:    228)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          36.0       1.5
          63.0       1.1
          76.0       1.4
          81.5       1.0
          82.0       1.3
          82.5       4.1
          83.0       1.3
          89.0       5.1
          91.0       2.8
          94.0       1.0
          94.5       3.2
          95.0       2.0
          95.5       4.0
          96.0       3.0
          96.5       1.1
         115.0      14.2
         116.0       2.0
         152.0       1.7
         165.0       4.9
         176.0       1.1
         178.0      15.6
         179.0       4.3
         189.0       6.2
         190.0       3.1
         191.0      17.8
         192.0      13.3
         193.0     100.0
         194.0      19.6
         195.0       1.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C15 H13 Cl 0.043 g : 0.5 ml CDCl3
    5-chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.44 to 7.02 B 6.093 C *1 3.73 D *1 2.97

         Hz     ppm     Int.
    

        662.50   7.398     93
        660.19   7.372    137
        659.13   7.360    118
        658.25   7.350     96
        656.69   7.333    191
        655.69   7.322    196
        652.75   7.289    379
        649.75   7.255    292
        648.81   7.245    356
        646.38   7.218    878
        645.38   7.207   1000
        643.81   7.189    643
        642.38   7.173    420
        640.50   7.152    240
        638.31   7.128    139
        635.19   7.093     73
        545.19   6.088    408
        351.31   3.923     82
        345.94   3.863     58
        341.56   3.814     97
        339.69   3.793    112
        335.50   3.747    118
        333.25   3.721    121
        326.75   3.649    128
        325.88   3.639    142
        321.00   3.585     59
        275.38   3.075    144
        274.19   3.062    123
        267.75   2.990    131
        265.50   2.965    119
        261.56   2.921    106
        259.50   2.898    110
        255.13   2.849     61
        249.63   2.788     74
    

KBr disc



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