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网站主页CAS数据库列表 100-76-5更多图谱奎宁环(100-76-5)红外图谱(IR2)

奎宁环

产品名称 奎宁环

CAS号100-76-5

分子式C7H13N

分子量111.18

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  • Mass

    MS-NW-7215          
    quinuclidine
    C7H13N              (Mass of molecular ion:    111)
    

       Source Temperature: 210 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       2.2
          26.0       1.0
          27.0       7.6
          28.0       5.4
          29.0       4.8
          30.0       2.0
          39.0       6.6
          40.0       1.3
          41.0      10.8
          42.0     100.0
          43.0       5.2
          44.0       1.2
          51.0       1.1
          53.0       3.8
          54.0       5.9
          55.0      19.7
          56.0       6.1
          57.0       8.8
          67.0       2.0
          68.0       5.5
          69.0      12.6
          70.0       2.5
          80.0       1.0
          81.0       2.4
          82.0      31.3
          83.0      13.4
          84.0       1.6
          96.0      19.7
          97.0       1.6
         110.0      17.8
         111.0      32.6
         112.0       2.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H13 N 0.034 g : 0.5 ml CDCl3
    quinuclidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.855 B 1.734 C 1.532 J(B,C)=3.2HZ. 90MHZ. : HSP-04-861

         Hz     ppm     Int.
    

       1159.91   2.903     57
       1159.55   2.902     57
       1149.05   2.876    936
       1141.24   2.856    953
       1138.92   2.850    687
       1133.30   2.836   1000
       1122.31   2.809     36
        703.13   1.760     34
        699.95   1.752    127
        696.66   1.744    298
        693.48   1.736    416
        690.31   1.728    341
        687.13   1.720    159
        683.96   1.712     42
        621.09   1.555    606
        617.80   1.546    653
        615.97   1.542    538
        612.55   1.533    780
        610.84   1.529    765
        605.47   1.516    658
        602.17   1.507    539
    


  • 1H NMR 89.56 MHz
    C7 H13 N 0.038 g : 0.5 ml CDCl3
    quinuclidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.847 B 1.74 C 1.53 400MHZ. : HSP-41-773

         Hz     ppm     Int.
    

        264.00   2.948    784
        256.31   2.862    925
        253.56   2.832    647
        248.50   2.775   1000
        242.94   2.713     81
        242.50   2.708     76
        240.69   2.688     59
        162.25   1.812     75
        159.13   1.777    174
        156.00   1.742    266
        152.94   1.708    283
        150.13   1.677    230
        145.75   1.628    656
        143.06   1.598    567
        141.06   1.576    525
        140.75   1.572    527
        140.44   1.569    525
        137.94   1.541    776
        130.50   1.458    581
        127.63   1.426    403
        123.13   1.375     67
    

in CDCl3



KBr disc



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